Sunan Abi Dawud — The Rites of Hajj (Kitab Al-Manasik Wa'l-Hajj) — Hadith No: 1896
Translation
Narrated Aisha, Ummul Mu'minin: The Companions of the Messenger of Allah (ﷺ) who accompanied him did not go round the Ka'bah till they threw pebbles at the Jamrah (pillar at Mina)